CN101199364A - Chinese herbal medicine cigarette filter tip rod for relieving cough and reducing sputum - Google Patents
Chinese herbal medicine cigarette filter tip rod for relieving cough and reducing sputum Download PDFInfo
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- CN101199364A CN101199364A CNA2006101254852A CN200610125485A CN101199364A CN 101199364 A CN101199364 A CN 101199364A CN A2006101254852 A CNA2006101254852 A CN A2006101254852A CN 200610125485 A CN200610125485 A CN 200610125485A CN 101199364 A CN101199364 A CN 101199364A
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- chinese herbal
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- reducing sputum
- cigarette filter
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Abstract
The invention discloses a cigarette filter rod which is added with Chinese herbal medicine and has the functions of relieving cough and eliminating phlegm, relating to a cigarette filter rod, in particular to a cigarette filter rod which is added with Chinese herbal medicine and has the functions of relieving cough and eliminating phlegm. The invention adopts the following technical scheme; Chinese herbal extracts with the functions of relieving cough and eliminating phlegm are added into the cigarette filter rod curing agent, the shaping paper and the tow material; the Chinese herbal extracts with the functions of relieving cough and eliminating phlegm are single extracts of folium ginkgo, Radix Peucedani, Radix Stemonae, sophora japonica and Japanese ardisia, respectively denoted with the code of E,N,P,U,S, or the combination of two of the above single extracts. The invention adds Chinese herbal medicine with the functions of relieving cough and eliminating phlegm into the cigarette filter rod and applies the principle of traditional Chinese fumigation treatment to enable the active ingredients of the Chinese herbal extracts to be transmitted into the smoke of the cigarette; the invention has obvious functions of relieving cough and eliminating phlegm and the added Chinese herbal extracts are in harmony with the taste of the cigarette, thus the invention can meet the requirements of the majority of the consumers.
Description
Technical field
The present invention relates to a kind of cigarette filter tip rod, especially a kind of cigarette filter tip rod that is added with Chinese herbal medicine with relieving cough and reducing sputum function.
Background technology
In the prior art, cigarette filter tip rod has been mature technology, and existing composite cigarette filter stick product appears on the market, and composite cigarette filter stick is to add non-fiber-like material such as carbon dust, silica gel etc. in filter rod, or in filter rod, add peppermint essence etc., thereby has certain specific function; But the interpolation material of this class filter tip and essence and cigarette sense organ hamony are not good, and the suction of cigarette flavor is brought in various degree negative effect, and consumer's acceptance level is lower.
Cigarette is obvious and outstanding to the harm performance of consumer's respiratory system, after in filter rod, adding relieving cough and reducing sputum Chinese herbal medicine and extract thereof, can reduce the harm of cigarette, domestic portioned product has added Chinese herbal medicine extract in cigarette, mainly adopt the tobacco perfuming mode that Chinese herbal medicine extract is added in the pipe tobacco.But these Chinese herbal medicine extracts participate in burning in cigarette, be not inconsistent with the conventional administering mode of Chinese herbal medicine, not only lose the corresponding function of medicine, and there is defective in the hamony of cigarette odor-absorbing and Chinese herbal medicine, product only adapts to the demand of a few consumers, regionality is stronger, is difficult to be fit to vast consumer's taste, is unfavorable for the development of brand.
Summary of the invention
Above-mentioned deficiency at prior art, the technical problem to be solved in the present invention provides a kind of relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod, it is added on Chinese herbal medicine extract in the filter rod, do not participate in burning, make Chinese herbal medicine be similar to the stifling administration of Chinese medicine, the function of medicine fully obtains performance, and has selected and the cigarette odor-absorbing Chinese herbal medicine and the dosage of harmony mutually, makes filter rod of the present invention be fit to consumers in general's demand.
Technical scheme of the present invention is: relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod has the identical outward appearance of regular-size cigarette filter rod, its special feature is: produce the curing agent of cigarette filter tip rod, forming paper, and strand material in add the relieving cough and reducing sputum Chinese herbal medicine extract, the folk prescription extract that described relieving cough and reducing sputum Chinese herbal medicine extract is ginkgo leaf, the root of purple-flowered peucedanum, the tuber of stemona, the sophora bud, ardisia japonica, represent with code name E, N, P, U, S respectively, or the combination compound extract of two above folk prescription extracts among them.
In the described combination compound extract, relieving cough and reducing sputum effect is obvious, and has with the good combination compound extract prescription of flue gas hamony:
Compound 1., E: N: P: U: S=1-2: 2-3.5: 1.5-4.5: 1.5-3: 1-2;
Compound 2., P: N=0.5-5: 0.5-3;
Compound 3., N: P: S=1-3: 2.5-6: 1-3;
Compound 4., P: S=2-5: 0.5-2;
Compound 5., E: N: P=1-2: 2.5-5: 3-6;
Compound 6., P: U=4-7: 1-3;
Compound 7., N: P: U=2.5-4: 3.5-6: 1-3;
Compound 8., P: U: S=3.5-6: 1-3: 1.5-3.
Described relieving cough and reducing sputum Chinese herbal medicine extract is Powdered or liquid.
Described interpolation relieving cough and reducing sputum Chinese herbal medicine extract, be meant by miscible, smear, spray with its attached to the curing agent of producing cigarette filter tip rod, forming paper, and strand material in, or in the filter rod strand material, add the carrier that contains the relieving cough and reducing sputum Chinese herbal medicine extract.
The described carrier that contains the relieving cough and reducing sputum Chinese herbal medicine extract that in the filter rod strand material, adds, be meant the carrier that can carry Chinese herbal medicine extract with a kind of, as fiber, cotton yarn class material, Chinese herbal medicine extract is adsorbed, is immersed in the carrier, this carrier that carries Chinese herbal medicine extract is wrapped among the strand material of filter rod
Chinese herbal medicine extract: the carrier=20-90wt% of carrying Chinese herbal medicine extract: 1.
The described relieving cough and reducing sputum Chinese herbal medicine that adds in curing agent is that Chinese herbal medicine extract is miscible with volume filter rod curing agent, and its miscible ratio is:
Relieving cough and reducing sputum Chinese herbal medicine extract: cigarette filter tip rod curing agent=0.1-1wt%: 1.
Aforesaidly be added with the volume filter rod curing agent of relieving cough and reducing sputum Chinese herbal medicine extract and the ratio of strand material is:
Be added with the volume filter rod curing agent of relieving cough and reducing sputum Chinese herbal medicine extract: strand material=4-9wt%: 1.
The described relieving cough and reducing sputum Chinese herbal medicine extract that adds in forming paper is to smear the relieving cough and reducing sputum Chinese herbal medicine extract on forming paper, and applying amount is 0.1g/m
2-3.0g/m
2
Technical measures of the present invention are reasonable, implement easily the relieving cough and reducing sputum Chinese herbal medicine extract to be added in the cigarette filter tip rod, adopt the principle of traditional Chinese medical science steaming therapy, and the relieving cough and reducing sputum Chinese herbal medicine effective ingredients is transferred in the cigarette smoke; Adopt the cigarette of filter rod of the present invention to have tangible relieving cough and reducing sputum function, reduce the harm of cigarette, consumer's respiratory system is played a protective role consumer's respiratory system; Simultaneously, the relieving cough and reducing sputum Chinese herbal medicine extract and the cigarette odor-absorbing of interpolation have good hamony, and cigarette odor-absorbing is not had a negative impact, and are a kind of novel products that can adapt to the most consumers demand.
The specific embodiment
Below technology path of the present invention and the other problem relevant with the present invention are described in further detail.The inventor has at first chosen 22 kinds of more rich relieving cough and reducing sputum Chinese herbal medicines of relievining asthma commonly used of crude drug in whole resource, and they are balloonflower root, loguat leaf, Chinese ephedra, semen armeniacae amarae, ginkgo leaf, the bulb of fritillary, tussilago, pericarpium citri grandis, Radix Glycyrrhizae, rhizoma pinellinae praeparata, polygala root, gynostemma pentaphylla, the sterculia seed, the root of purple-flowered peucedanum, Sang Baipi, the tuber of stemona, tarragon, gynostemma pentaphylla, ardisia japonica, tealeaves, bud of japanese pagoda tree, marine alga.According to the known performance of the prior art of medicine, and the extracting method of this medicine in the prior art, make 22 kinds of Chinese herbal medicine folk prescription extracts.Main chemical compositions to above Chinese herbal medicine extract sample is analyzed, medical consumption per day and physicochemical characteristics according to this medicine, be combined into the compound of various folk prescription extracts, these folk prescriptions and compound are applied in the filter rod with various adding proportions, the cigarette that is added with Chinese herbal medicine extract in the filter rod is carried out sensory quality assessment and pharmacology and toxicological security evaluation (adopting the method for prior art), determine the reasonable usage ratio of extract, harmony per sample and sensory evaluation result carry out repetitious compatibility test, it is good to choose with cigarette harmony, no obvious and offending Chinese herbal medicine breath is to improving Chinese herbal medicine extract folk prescription and the compound that the cigarette mouthfeel has certain effect.Finally chosen the folk prescription extract of ginkgo leaf, the root of purple-flowered peucedanum, the tuber of stemona, the sophora bud, ardisia japonica five kinds of medicines, represent with code name E, N, P, U, S respectively, with the compound that two or more folk prescription extracts in them fit in, the folk prescription extract of five kinds of above-mentioned medicines and their compound are exactly relieving cough and reducing sputum Chinese herbal medicine extract of the present invention.
The extracting method and the performance division of the folk prescription extract of ginkgo leaf, the root of purple-flowered peucedanum, the tuber of stemona, the sophora bud, five kinds of medicines of ardisia japonica are as follows:
1, the preparation of ginkgo biloba p.e and technology: taking by weighing the ginkgo leaf meal, make solvent with 70% ethanol, is under 100 ℃ of conditions at bath temperature, distillation and reflux extracted 2 hours, with 10 times of water gagings (weight with the medicine meal is datum quantity, and is as follows), filter for the first time; The dregs of a decoction are used 6 times of water gagings again, extract 2 hours, filter, merge gained filtrate twice, decompression recycling ethanol is dissolved in water to small size, and the pH value of solution value transfers to pH9-10, leave standstill, inclining top clear liquid, and the suction filtration precipitation uses the distilled water washing and precipitating to pH5-6, precipitation is dried to powdery or is mixed with 1% (mass ratio) solution with analyzing pure propane diols, promptly get ginkgo biloba p.e folk prescription (code name is E); This folk prescription has covers assorted gas, improves flue gas concentration, and the cough due to deficiency of the lung is had the improvement effect.Its main active ingredient is ginkgolides (Ginkgolides); Its chemical structural formula is as follows:
Ginkgolides
2, the preparation of Radix Peucedani extract and technology: get root of purple-flowered peucedanum medicinal material coarse powder, make solvent with 60-90 ℃ of benzinum, distillation and reflux extracts 2 times, extracts 2 hours with 2.5 times of amount benzinums for the first time, filters while hot; Filter residue extracted 1 hour with 2.5 times of amount benzinums again, filtered while hot; Merge gained filtrate twice, the recovered under reduced pressure benzinum after being dissolved in water, is being no more than filtration drying under 100 ℃ of temperature to small size, makes powdered or is mixed with 1% solution with analyzing pure propane diols.Be Radix Peucedani extract folk prescription (code name is N); This folk prescription has obvious minimizing respiratory secretions, phlegm-dispelling functions; Can make flue gas finer and smoother, soft, improve flue gas concentration.Its main active ingredient is root of purple-flowered peucedanum first element; Its chemical structural formula is as follows:
3, the preparation of Radix Stemonae extract and technology: get tuber of stemona medicinal material coarse powder, make solvent with 95% ethanol, distillation and reflux extracts 2 times, measures alcohol extracts 2 hours with 2.5 times for the first time, filters, the dregs of a decoction extracted 1.5 hours with 2 times of amount ethanol 1.5 again, filter, merge gained filtrate twice, decompression recycling ethanol is to small size, concentrate drying is mixed with 1% solution to powdery or with analyzing pure propane diols, promptly gets Radix Stemonae extract folk prescription (code name is P); This folk prescription has soft flue gas, improves mouthfeel; Effects such as loose bronchial smooth muscle.Its main active component is stemonine (Stemonine); Its chemical structural formula is as follows:
4, the preparation of sophora bud extract and technology: get sophora bud medicinal material coarse powder, the clarification saturated limewater heating that adds 10 times of amounts was boiled 15 minutes, filtered while hot, and residue boiled 10 minutes with the heating of 7 times of amount clarification saturated limewaters again, filtered while hot.Merge filtrate twice, adjust filtrate to pH3-4 with HCl, leave standstill, leach supernatant, the suction filtration precipitation is washed till pH5-6 with distilled water, and the operation that repeats above-mentioned adjust pH once with 70 ℃ of temperature dryings, is got dried powder 2%H
2SO
4, refluxed 2 hours, filter, be washed till pH5-6 with distilled water, make behind 80 ℃ of temperature dryings for powdery or with analyzing pure propane diols and be mixed with 1% solution, promptly get sophora bud extract folk prescription (code name is U); This folk prescription has fine and smooth flue gas, improves flue gas concentration, antiasthmatic effect.Its main active ingredient is Quercetin (Quercetin); Its chemical structural formula is as follows:
5, the preparation of ardisia japonica extract and technology: get the ardisia japonica medicinal material coarse powder, boil three times with the decocting of 6 times of amounts, each 1 hour, merge decocting liquid, filter, be concentrated into the thick paste shape; 2 times of amount 95% ethanol with the thick paste quality are pinched molten thick paste to the loose particles shape, three times repeatedly, filter, merge gained filtrate, it is an amount of to add concentrated ammonia liquor, making filtrate is pH9-10, and sedimentation and filtration is with 95% ethanol washing and precipitating, merging filtrate and washing lotion, decompression recycling ethanol, concentrate drying is mixed with 1% solution to powdery or with analyzing pure propane diols, promptly gets ardisia japonica extract folk prescription (code name is S); This folk prescription makes that the flue gas exquisiteness is soft, mouthfeel is improved, and has significantly Antitussive and Expectorant Effect.Its main active ingredient is Bergenin (Bergenin); Its chemical structural formula is as follows:
Embodiment 1
Using compound Chinese herbal medicine extract 1. is immersed in the cotton, making the content of Chinese herbal medicine extract in cotton is 55wt%, this cotton is wrapped in the strand material of cigarette filter tip rod, the employing conventional equipment is produced, make the specification filter rod the same with common filter rod with outward appearance, and (this cigarette shreds is a Wuhan tobacco group medium and high-grade goods finished cut tobacco to be applied to cigarette, as follows), to contain the cigarette and the contrast of former finished cigarettes of Chinese herbal medicine extract, carry out sense organ contrast evaluation by the method for prior art.Evaluation result is:
1, sense of smell: faint medicine perfume (or spice) is arranged, cigarette table perfume (or spice) is had no adverse effects basically.
2, sensory evaluating smoking: cigarette flavor is not had obvious negative effect, faint medicine perfume (or spice) is arranged, and harmony is good, the soft degree of flue gas improves, concentration slightly increases, and the oral cavity is residual slightly to be increased, and the aftertaste sense strengthens.
Embodiment 2
Using compound Chinese herbal medicine extract 2. spreads upon it on yew paper, the coating consumption is 0.55g/m2, the filter rod specification is 100mm * 24.2mm (length * circumference), this filter rod that scribbles Chinese herbal medicine extract is applied to cigarette, to contain the cigarette and the contrast of former finished cigarettes of Chinese herbal medicine extract, carry out sense organ contrast evaluation by the method for prior art.Evaluation result is:
1, the sense of taste: cigarette props up filter end does not have obvious peculiar smell.
2, sense of smell: faint medicine perfume (or spice) is arranged, cigarette table perfume base is originally had no adverse effects.
3, sensory evaluating smoking: except that smelling fragrant slightly faint medicine perfume (or spice), the aesthetic quality does not have significant change to cigarette.
Embodiment 3
Using compound Chinese herbal medicine extract 3. sprays it in the filter rod curing agent, the curing agent that uses during the filter rod moulding is a triacetyl glycerine, compound relieving cough and reducing sputum Chinese herbal medicine extract 3. is evenly miscible in wherein, the ratio of applying is " Chinese herbal medicine extract: curing agent=0.5wt%: 1 ", and the curing agent after the preparation and the application percentage of strand material can be that the 7wt% of strand material nurses one's health by curing agent according to designing requirements such as filter stick hardness and resistance to suctions.This filter rod that contains Chinese herbal medicine extract is applied to cigarette, will contains the cigarette and the contrast of former finished cigarettes of Chinese herbal medicine extract, carry out sense organ contrast evaluation by the method for prior art.Evaluation result is:
1, the sense of taste: cigarette props up filter end does not have obvious peculiar smell.
2, sense of smell: faint medicine perfume (or spice) is arranged, to the fragrant no obvious negative effect of cigarette table.
3, sensory evaluating smoking: fragrance is sent out thoroughly, and hamony is good, and flue gas is more plentiful, and the aftertaste sense strengthens.
Simply introduce other several embodiment such as following table below:
Table 1 embodiment and effect
Embodiment number | Compound and proportioning | Effect |
4 | E: N: P=2: 3: 5 | Minimizing expectoration, throat feel comfortably cool, and hamony is good, the residual increase in oral cavity. |
5 | E: N: P=2: 5: 3 | Minimizing expectoration, throat feel comfortably cool, and hamony is good, and fragrance is covered. |
6 | P: U=7: 3 | Relieving asthma, throat feels comfortably cool, hamony is good, concentration stimulates and increases. |
7 | N: P: S=1.5: 5.5: 3 | Kobadrin, hamony is good, the residual increase in oral cavity. |
8 | N: P: U=3: 5: 2 | Antitussive and antiasthmatic, hamony is good, and concentration stimulates and increases. |
9 | P: U: S=4: 3: 3 | Kobadrin, throat feel comfortably cool, and hamony is good, and concentration stimulates and increases. |
The present invention adopts the principle of traditional Chinese medical science steaming therapy, relieving cough and reducing sputum active ingredient is transferred in the cigarette smoke, adopts the HPLC detection method, can from cigarette smoke, detect the active ingredient of folk prescription and compound, 1. with compound is example, and the detection level of its main component in flue gas is as shown in table 2 below:
Main effectively composition detection result in table 2 cigarette smoke
Annotate: 1. the puff number of cigarette and TPM are respectively 7.31 mouthfuls and 19.54mg/ and prop up.
2. μ g/cig refers to that every cigarette contains certain material μ g amount.
Have tangible relieving cough and reducing sputum function according to detecting the susceptible of proof cigarette, reduce the harm of cigarette, consumer's respiratory system is played a protective role consumer's respiratory system; Simultaneously, the relieving cough and reducing sputum Chinese herbal medicine extract compound and the cigarette odor-absorbing of interpolation have good hamony, and cigarette odor-absorbing is not had a negative impact.
The functional filter stick of above-mentioned relieving cough and reducing sputum Chinese herbal medicine adopts conventional equipment production, and its specification is consistent with conventional filtration mouth rod, and length * circumference is about (90mm---132mm) * (18.0mm---25.0mm); The resistance to suction of filter rod is stipulated by the cigarette designing requirement.
The functional filter stick of above-mentioned relieving cough and reducing sputum Chinese herbal medicine is easy to process, does not change existing filter rod manufacturing process technology and major technology index generally, does not influence the presentation quality of cigarette product, can also increase the antiforge function of product.Be adapted to exploitation of filter stick and cigarette and production.
Claims (8)
1. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod, has the identical outward appearance of regular-size cigarette filter rod, it is characterized in that: produce the curing agent of cigarette filter tip rod, forming paper, and strand material in add the relieving cough and reducing sputum Chinese herbal medicine extract, the folk prescription extract that described relieving cough and reducing sputum Chinese herbal medicine extract is ginkgo leaf, the root of purple-flowered peucedanum, the tuber of stemona, the sophora bud, ardisia japonica, represent with code name E, N, P, U, S respectively, or the combination compound extract of two above folk prescription extracts among them.
2. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 1 is characterized in that: in the described combination compound extract, relieving cough and reducing sputum effect is obvious, and has with the good combination compound extract prescription of flue gas hamony:
Compound 1., E: N: P: U: S=1-2: 2-3.5: 1.5-4.5: 1.5-3: 1-2;
Compound 2., P: N=0.5-5: 0.5-3;
Compound 3., N: P: S=1-3: 2.5-6: 1-3;
Compound 4., P: S=2-5: 0.5-2;
Compound 5., E: N: P=1-2: 2.5-5: 3-6;
Compound 6., P: U=4-7: 1-3;
Compound 7., N: P: U=2.5-4: 3.5-6: 1-3;
Compound 8., P: U: S=3.5-6: 1-3: 1.5-3.
3. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 1 is characterized in that: described relieving cough and reducing sputum Chinese herbal medicine extract is Powdered or liquid.
4. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 1, it is characterized in that: described interpolation relieving cough and reducing sputum Chinese herbal medicine extract, be meant by miscible, smear, spray with its attached to the curing agent of producing cigarette filter tip rod, forming paper, and strand material in, or in the filter rod strand material, add the carrier that contains the relieving cough and reducing sputum Chinese herbal medicine extract.
5. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 4, it is characterized in that: the described carrier that contains the relieving cough and reducing sputum Chinese herbal medicine extract that in the filter rod strand material, adds, be meant the carrier that can carry Chinese herbal medicine extract with a kind of, as fiber, cotton yarn class material, Chinese herbal medicine extract is adsorbed, is immersed in the carrier, this carrier that carries Chinese herbal medicine extract is wrapped among the strand material of filter rod
Chinese herbal medicine extract: the carrier=20-90wt% of carrying Chinese herbal medicine extract: 1.
6. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 1 is characterized in that: the described relieving cough and reducing sputum Chinese herbal medicine that adds in curing agent is that Chinese herbal medicine extract is miscible with volume filter rod curing agent, and its miscible ratio is:
Relieving cough and reducing sputum Chinese herbal medicine extract: cigarette filter tip rod curing agent=0.1-1wt%: 1.
7. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 6 is characterized in that: aforesaidly be added with the volume filter rod curing agent of relieving cough and reducing sputum Chinese herbal medicine extract and the ratio of strand material is:
Be added with the volume filter rod curing agent of relieving cough and reducing sputum Chinese herbal medicine extract: strand material=4-9wt%: 1.
8. relieving cough and reducing sputum Chinese herbal medicine cigarette filter tip rod according to claim 1 is characterized in that: the described relieving cough and reducing sputum Chinese herbal medicine extract that adds in forming paper is to smear the relieving cough and reducing sputum Chinese herbal medicine extract on forming paper, and the amount of smearing is 0.1g/m
2-3.0g/m
2
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CNA2006101254852A CN101199364A (en) | 2006-12-15 | 2006-12-15 | Chinese herbal medicine cigarette filter tip rod for relieving cough and reducing sputum |
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CN102090719A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, strengthening body, relieving cough and moisturizing throat |
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CN102090718A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, relieving cough and refreshing |
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US8143738B2 (en) | 2008-08-06 | 2012-03-27 | Infinite Wind Energy LLC | Hyper-surface wind generator |
CN102090719A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for protecting health, strengthening body, relieving cough and moisturizing throat |
CN102090721A (en) * | 2010-09-15 | 2011-06-15 | 张锐 | Cigarette filtering agent for health care and cough relief |
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CN102090721B (en) * | 2010-09-15 | 2013-06-05 | 程卫国 | Cigarette filtering agent for health care and cough relief |
CN103082413A (en) * | 2011-11-08 | 2013-05-08 | 江西中烟工业有限责任公司 | Method for decreasing cigarette offensive odor by utilizing composite Chinese herbal medicine |
CN104153255A (en) * | 2014-07-29 | 2014-11-19 | 安徽省三环纸业(集团)有限公司 | Unprocessed rehmannia root and tortoise shell health aroma type tipping paper with high tensile strength and preparation method thereof |
CN106165907A (en) * | 2016-07-28 | 2016-11-30 | 福建中烟工业有限责任公司 | A kind of cigarette filter rod containing Thuja extract |
CN107022415A (en) * | 2017-04-27 | 2017-08-08 | 河南中烟工业有限责任公司 | A kind of quick-fried pearl boat-fruited sterculia essence of cigarette and its application in cigarette |
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